;noesyhsl1tp.val ;2D homonuclear correlation via dipolar coupling ;dipolar coupling may be due to noe or chemical exchange. ;phase sensitive using TPPI ;with homospoil pulses in mixing time ; ; val mar4,'98 ; http://nmr.ioc.ac.ru/Staff/AnanikovVP/ ; #include "p2=2*p1" "d0=3u" "d20=50m" "d8=l1*d20" 1 ze 2 d1 3 p1 ph1 d0 p1 ph2 30u LOCKH_ON 4 3u HS_ON 150u 3u HS_OFF d20 d16 lo to 4 times l1 10u LOCKH_OFF p1 ph3 go=2 ph31 d1 wr #0 if #0 id0 ip1 zd lo to 3 times td1 exit ph1=0 2 ph2=0 0 ph3=0 ph4=0 ph31=0 2 ;pl1 : f1 channel - power level for pulse (default) ;p1 : f1 channel - 90 degree high power pulse ;d0 : incremented delay (2D) = 3u ;d1 : relaxation delay; 1-5 * T1 ;l1 : number of steps, i.e. d8=d20*l1 ;d8 : l1*d20 - mixing time; for compatibility only, do not input ;d16: delay for homospoil recovery ;d20: step size; =50m, change if needed ;in0: 1/(2 * SW) = DW ;nd0: 2 ;NS: 2 * n ;DS: 16 ;td1: number of experiments ;MC2: TPPI ;!!!!!!! Example !!!!!!!! , d20=50m, l1=7 (d8=350m) ;GCB Settings Overview: ; ;Output: SCB-R ;Shape: Sine ;Sequence: 1234567 ;Compensation 1: Amplitude = 0 Tau = 0 us ;Compensation 2: Amplitude = 0 Tau = 0 us ;Compensation 3: Amplitude = 0 Tau = 0 us ; ;Pulse Amplitude PulseDuration CompensationDuration Increment ; 1 2000 50000 us 0 us 0 ; 2 2000 50000 us 0 us 0 ; 3 2000 50000 us 0 us 0 ; 4 2000 50000 us 0 us 0 ; 5 2000 50000 us 0 us 0 ; 6 2000 50000 us 0 us 0 ; 7 2000 50000 us 0 us 0 ; 8 0 300 us 0 us 0 ; 9 0 300 us 0 us 0 ;10 0 300 us 0 us 0 ;11 0 300 us 0 us 0